摘要
目的:研究无梗五加[Acanthopanax sessiliflorus(Ruqr.et Maxim)Seem.]果实的化学成分。方法:采用溶剂提取法、溶剂萃取法、硅胶柱层析法、凝胶柱层析法、重结晶法对无梗五加果实中的化合物进行分离纯化;根据光谱数据和理化性质确定化合物结构。结果:分离并鉴定了6个化合物,分别为:chiisanogenin(1),东莨菪内酯(2),胡萝卜苷棕榈酸酯(3),东莨菪苷(4),丁二酸(5),卫矛醇(6)。结论:化合物3、5、6为首次从无梗五加果实中分离得到。
Objective： To study the chemical constituents of the fruits of Acanthopanax sessiliflorus（Ruqr.et Maxim）Seem.Method：The methods of solvent extraction,silica gel column,Sephadex LH-20 column and recrystallizition were used for the isolation and spectroscopy methods were used for the structure identification.Results：6 compounds were isolated.They were identified as chiisanogenin（1）,scopoletin（2）,daucosterol palmitate（3）,scopolin（4）,succinate（5）,galactitol（6）.Conclusion：Compounds 3,5 and 6 were isolated from the fruits of Acanthopanax sessiliflorus（Ruqr.et Maxim）Seem.for the first time.
出处
《中华中医药学刊》
CAS
2012年第4期772-773,共2页
Chinese Archives of Traditional Chinese Medicine
基金
辽宁省自然科学基金资助项目(20102147)
关键词
无梗五加
化学成分
结构鉴定
Acanthopanax sessiliflorus
chemical constituent
structure identific ation
