摘要
建立了一种以0.005 mol/L硫酸为萃取剂、高效液相色谱法同时测定卷烟纸中柠檬酸根、酒石酸根、苹果酸根、乳酸根、琥珀酸根及富马酸根的方法,并采用该方法测定了18种卷烟纸样品。结果表明：①这6种有机酸根的平均回收率为91.64%~105.09%,相对标准偏差≤2.65%;②18种卷烟纸样品中柠檬酸根、酒石酸根、苹果酸根、乳酸根、琥珀酸根和富马酸根含量范围分别为6.03~24.45,0~8.13,0~6.91,0~0.98,0~0.31和0~0.1 mg/g。
A method for simultaneously determining the citric,tartaric,malic,lactic,succinic,and fumaric anions in cigarette paper was developed by extraction with 0.005 mol/L sulfuric acid solution and separation by HPLC.18 cigarette paper samples were tested with the developed method,the results showed that： 1） the average recoveries of the six organic acidic anions ranged from 91.64% to 105.09%,with RSDs of ≤2.65%;2） the contents of citric,tartaric,malic,lactic,succinic,and fumaric anions in samples ranged from 6.03 to 24.45,0 to 8.13,0 to 6.91,0 to 0.98,0 to 0.31,and 0 to 0.1 mg/g,respectively.
出处
《烟草科技》
EI
CAS
北大核心
2010年第5期34-37,共4页
Tobacco Science & Technology
基金
四川省科学技术厅基金项目"川渝销区卷烟特征剖析"(2008JY0142)
关键词
高效液相色谱法
卷烟纸
有机酸根
High performance liquid chromatography（HPLC）
Cigarette paper
Organic acid
Acidic anion
