摘要
采用碳酸乙烯酯作萃取剂萃取精馏分离碳酸二甲酯(DMC)与甲醇的恒沸物,为了得到纯度达99.5%的DMC产品,利用ASPEN PLUS流程模拟软件对此过程进行了模拟计算,得到了最佳的工艺操作条件及工艺参数,DMC的纯度达到99.67%,萃取剂可以完全循环利用,为工业化装置提供了重要的理论依据和设计参考。
Ethylene carbonate was used as extractant for the separation of dimethyl carbonate - methanol azeo- trope by extractive distillation. In order to obtain the purified DMC (99.5%), ASPEN PLUS software was used to simulate the separation process, and the optimum operation conditions and process parameters were obtained. The purity of dimethyl carbonate product was 99.67% and ethyl carbonate extractant could be recycled completely in this separation process. The results could be used as the theoretical basis and design reference for industrial apparatus.
出处
《天然气化工—C1化学与化工》
CAS
CSCD
北大核心
2007年第5期19-22,共4页
Natural Gas Chemical Industry