The microstructural evolution of AZ91D magnesium alloy prepared by means of the cyclic upsetting-extrusion and partial remelting was investigated. The effects of remelting temperature and holding time on microstructur...The microstructural evolution of AZ91D magnesium alloy prepared by means of the cyclic upsetting-extrusion and partial remelting was investigated. The effects of remelting temperature and holding time on microstructure of semi-solid AZ91D magnesium alloy were studied. Furthermore, tensile properties of thixoextruded AZ91D magnesium alloy components were determined. The results show that the cyclic upsetting-extrusion followed by partial remelting is effective in producing semi-solid AZ91D magnesium alloy for thixofonning. During the partial remelting, with the increase of remelting temperature and holding time, the solid grain size increases and the degree of spheroidization tends to be improved. The tensile mechanical properties of thixoextruded AZ91D magnesium alloy components produced by cyclic upsetting-extrusion and partial remelting are better than those of the same alloy produced by casting.展开更多
The effects of Al-8B grain refiner on microstructure and tensile properties of an Al-12Zn-3Mg-2.5Cu alloy produced by modified strain induced melt activation process were investigated. Pre-deformation of 60% was used ...The effects of Al-8B grain refiner on microstructure and tensile properties of an Al-12Zn-3Mg-2.5Cu alloy produced by modified strain induced melt activation process were investigated. Pre-deformation of 60% was used by hot working at 300 ℃. After pre-deformation, the samples were heated to a temperature above the solidus and below the liquidus point and maintained in the isothermal conditions at three different temperatures（500, 550 and 590 ℃） for varying time（10, 20 and 40 min）. It was observed that strain induced melt activation has caused the globular morphology of α（Al） grains. Microstructural study was carried out on the alloy by using optical microscope and scanning electron microscope in both unrefined and B-refined conditions. The results showed that for the desired microstructures of the alloy during SIMA process, the optimum temperature and time are 550 ℃ and 10 min, respectively. After the T6 heat treatment, the average tensile strengths increased from 278 to 585 MPa and 252 to 560 MPa for samples refined with 3.75% Al-8B before and after SIMA process, respectively. The ultimate strength of SIMA specimens is lower than that of B-refined specimens.展开更多
Tensile fracture behaviors of thixocast, artificially aged thixocast （thixocast＋T6） and as-extruded AA7075 alloys were investigated. The microstructural and fractographic observations were carried out using optical...Tensile fracture behaviors of thixocast, artificially aged thixocast （thixocast＋T6） and as-extruded AA7075 alloys were investigated. The microstructural and fractographic observations were carried out using optical microscope （OM） and scanning electron microscope （SEM）. Experimental studies showed that as-extruded and thixocast＋T6 specimens exhibited considerably more excellent mechanical properties than as-thixocast AA7075 specimen. T6 artificial heat treatment with prolonged solution treatment significantly improved the tensile properties of the thixocast AA7075 alloy. The tensile properties of as-extruded and thixocast＋T6 specimens were close to each other. In as-thixocast specimen having remarkable micro-cracks, fracture was intergranular brittle type. The ductile fracture surfaces were observed in as-extruded and thixocast＋T6 specimens. In as-thixocast specimens, decohesion started between the eutectic-matrix interfaces and propagated through grains. Micro-void coalescence was the dominant form of fracture in thixocast＋T6 heat treated specimens. The micro-voids nucleation was initiated at the interface between the matrix and multinary eutectic structure.展开更多
文摘The microstructural evolution of AZ91D magnesium alloy prepared by means of the cyclic upsetting-extrusion and partial remelting was investigated. The effects of remelting temperature and holding time on microstructure of semi-solid AZ91D magnesium alloy were studied. Furthermore, tensile properties of thixoextruded AZ91D magnesium alloy components were determined. The results show that the cyclic upsetting-extrusion followed by partial remelting is effective in producing semi-solid AZ91D magnesium alloy for thixofonning. During the partial remelting, with the increase of remelting temperature and holding time, the solid grain size increases and the degree of spheroidization tends to be improved. The tensile mechanical properties of thixoextruded AZ91D magnesium alloy components produced by cyclic upsetting-extrusion and partial remelting are better than those of the same alloy produced by casting.
基金Project(51175018) supported by the National Natural Science Foundation of ChinaProject(HIT.NSRIF2010118) supported by the Fundamental Research Funds for the Central Universities, China
文摘The effects of Al-8B grain refiner on microstructure and tensile properties of an Al-12Zn-3Mg-2.5Cu alloy produced by modified strain induced melt activation process were investigated. Pre-deformation of 60% was used by hot working at 300 ℃. After pre-deformation, the samples were heated to a temperature above the solidus and below the liquidus point and maintained in the isothermal conditions at three different temperatures（500, 550 and 590 ℃） for varying time（10, 20 and 40 min）. It was observed that strain induced melt activation has caused the globular morphology of α（Al） grains. Microstructural study was carried out on the alloy by using optical microscope and scanning electron microscope in both unrefined and B-refined conditions. The results showed that for the desired microstructures of the alloy during SIMA process, the optimum temperature and time are 550 ℃ and 10 min, respectively. After the T6 heat treatment, the average tensile strengths increased from 278 to 585 MPa and 252 to 560 MPa for samples refined with 3.75% Al-8B before and after SIMA process, respectively. The ultimate strength of SIMA specimens is lower than that of B-refined specimens.
基金the financial supports of the State Planning Organization of Turkey (DPT Project Number: 2003K120470-27)Gazi University Scientific Research Fund (GUBAP Project Number: 07/2013-01)
文摘Tensile fracture behaviors of thixocast, artificially aged thixocast （thixocast＋T6） and as-extruded AA7075 alloys were investigated. The microstructural and fractographic observations were carried out using optical microscope （OM） and scanning electron microscope （SEM）. Experimental studies showed that as-extruded and thixocast＋T6 specimens exhibited considerably more excellent mechanical properties than as-thixocast AA7075 specimen. T6 artificial heat treatment with prolonged solution treatment significantly improved the tensile properties of the thixocast AA7075 alloy. The tensile properties of as-extruded and thixocast＋T6 specimens were close to each other. In as-thixocast specimen having remarkable micro-cracks, fracture was intergranular brittle type. The ductile fracture surfaces were observed in as-extruded and thixocast＋T6 specimens. In as-thixocast specimens, decohesion started between the eutectic-matrix interfaces and propagated through grains. Micro-void coalescence was the dominant form of fracture in thixocast＋T6 heat treated specimens. The micro-voids nucleation was initiated at the interface between the matrix and multinary eutectic structure.
