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气相色谱法测定乳粉中亚油酸 被引量:9

The Determination of LA in Milk Powder by GC
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摘要 用改良的罗兹-哥特里法提取脂肪,然后将样品进行甲酯化,以3%OV-101色谱柱用气相色谱法测定亚油酸。结果:LA的回收率为97.1%—103.3%,RSD为1.53%。应用本方法测定乳制品中的亚油酸,具有操作简单、精密度高、重现好等特点。 In this paper, fat was extracted by improved Rose-Gottlieb method. After esterification the LA was determined by GC with the column of 3% OV-101. The results were that recoveries of LA was 97.1%-103.3%, relative standard deviation was 1.53%. If the method of determination of LA in milk powder in this paper was applied, the loss of LA would be reduced and the results would be satisfactory.
出处 《乳业科学与技术》 2002年第4期16-18,共3页 JOURNAL OF DAIRY SCIENCE AND TECHNOLOGY
关键词 亚油酸 气相色谱法 乳粉 罗兹-哥特里法 含量测定 Linoleic acid (LA) Gas chromatography Milk powder Rose-Gottlieb method
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