摘要
综述了不同水产品(无脊椎动物、贝类、鱼类、海鸟、哺乳动物等)样品中全氟化合物(PFCs)的提取方法(有机溶剂-水提取、碱性消化提取、离子对液液提取、加压液体萃取以及超声萃取)、净化方法(二氧化硅柱层析、分散石墨化碳和/或弱阴离子交换固相萃取、混合模式固相萃取;QuEChERS或分散固相萃取;反向液液萃取;凝胶渗透色谱;低温冷冻去脂)、测定方法[超高效液相色谱-串联质谱法(UPLC-MS/MS)、湍流色谱-串联质谱法(TFC-MS/MS)、纳升液相色谱-串联质谱法(nano LC-MS/MS)、超高效液相色谱-飞行时间-质谱法(UPLC-TOF-MS)]和分布物征的研究进展,并对其进行了展望(引用文献76篇)。
Research progress of extracting methods(organic solvent-water extraction,alkaline digestion extraction,ion-pair liquid-liquid extraction,pressurized liquid extraction and ultrasonic extraction),purification methods(silica column chromatography,dispersed graphitized carbon and/or weak anion exchange solid phase extraction,mixed mode solid phase extraction,QuEChERS or dispersed solid phase extraction,reverse liquid-liquid extraction,gel permeation chromatography,low-temperature freezing degreasing),determination methods(UPLCMS/MS,TFC-MS/MS,nano LC-MS/MS,UPLC-TOF-MS)and distribution characteristics of the perfluorinated compounds in samples of different aquatic products(invertebrates,shellfish,fish,seabirds mammals,etc)were reviewed,and prospects were made for it(76references cited).
作者
李佩佩
龙举
方益
严忠雍
张小军
LI Peipei;LONG Ju;FANG Yi;YAN Zhongyong;ZHANG Xiaojun(Key Lab of Sustainable Utilization of Technology Research for Fishery Resource of Zhejiang Province,Marine Fisheries Research Institute of Zhejiang,Zhoushan 316021,China)
出处
《理化检验（化学分册）》
CAS
CSCD
北大核心
2020年第6期735-744,共10页
Physical Testing and Chemical Analysis(Part B:Chemical Analysis)
基金
浙江省自然科学基金项目(LY17C200009)
浙江省科技项目(2017F10018)。
关键词
全氟化合物
水产品
前处理方法
测定方法
分布特征
综述
perfluorinated compound
pretreatment method
determination method
distribution characteristic
review
