摘要
以汉中地产橘皮为原料,进行草酸铵法和混合盐析法橘皮果胶提取工艺条件的对比研究。实验结果表明,草酸铵法在浸提温度80℃、草酸铵浓度0.8%、料液比1∶30、浸提时间1.5h的最佳工艺条件下,果胶产率为35.6%;混合盐析法在浸提温度80℃、混合盐比12∶1、浸提时间1.5h、pH3.8的最佳工艺条件下,果胶产率为8.1%。因此,我们建议工业上用草酸铵法来提取果胶。
Applied local orange peel in Hanzhong as experimental material, the comparison extracted research of pectin from orange peel by ammonium oxalate and mixing-salting out methods was carried out. The results showed that by ammonium oxalate method, un- der the best extraction process conditions of extraction temperature 80℃, ammonium oxalate mass fraction 0.8%, the ratio of solvent to material 1 : 30 and extraction time 1.5h, the pectin yield was 35.6%, while the pectin extraction rate was 8.1% by mixing-salting out method under the extraction temperature 80℃, the ratio of mixing-salt 12 : 1, solvent to material ratio 1 : 30, extraction time 1.5h and pH value 7. So ammonium oxalate was suggested to be used in industrial extraction of pectin from orange peel.
出处
《化工技术与开发》
CAS
2013年第7期15-17,共3页
Technology & Development of Chemical Industry
基金
陕西省教育厅科学研究项目(12JK0637)
陕西省科学技术厅项目(2011k17-03-10)
关键词
橘皮
草酸铵
混合盐析
果胶
提取
产率
orange peel
ammonium oxalate
mixing-salting out
pectin
extraction
yield