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顶空固相微萃取-气相色谱-质谱法测定发酵糯玉米黏豆包挥发性风味物质 被引量:3

Identification of volatile compounds in glue ball of fermented waxy corn using headspace solid-phase icroextraction gas chromatograph-mass spectrometry(HS-SPME-GC-MS)
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摘要 采用顶空固相微萃取法和气相色谱-质谱联用分析技术,对不同乳酸菌发酵的糯玉米黏豆包A和B中挥发性风味化合物进行分离鉴定。在黏豆包A和B中分别鉴定出60种和56种挥发性风味化合物,分析结果表明,其挥发性物质包括有机酸、酯类、醛类、酮类、醇类、酚类、醚类、烃类及杂环类等11类60多种化合物。初步认为1-甲基-2-苯咪唑啉酮、丁酸、月桂酸、丙醇、2,4,6-三甲基苯甲醛、壬醛、茴香脑、己酸己酯、肉豆蔻酸甲酯、棕榈酸甲酯等含量较高成份为糯玉米黏豆包的特征风味物质。 The waxy corn of glue ball were fermented by lactobacillus,and the volatile flavor components in two kids of glue corn absorbed with headspace solid-phase microextraction were analyzed by gas chromatograph-mass spectrometry GC/MS.The 60 compounds in corn glue ball A and 56 compounds in glue ball B were indentied as volatile flavors,included organic acids,esters,aldehydes,ketones,alcohols,phenols,ethers,hydrocarbon and heterocyclics,total 60 components with 11 varieties.The characteristic volatile flavors in waxy corn of glue ball were 1,3-dihydro-1-methyl-2H-Benzimidazol-2-one,Butanoic acid,Lauric acid,propanol,mesitaldehyde,nonanal,1-methoxy-4-(1-propenyl)-benzene,hexyl hexanoate,methyl tetrade-canoate,hexadecanoic acid methyl ester.
出处 《食品科技》 CAS 北大核心 2011年第4期269-275,共7页 Food Science and Technology
关键词 糯玉米 黏豆包 挥发性风味物质 顶空固相微萃取 气相色谱-质谱法 waxy corn glue ball volatile flavor components headspace solid-phase microextraction gas chromatography-mass spectrometry
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