摘要
以苯胺和顺酐为主要原料合成耐热改性剂N－苯基马来酰亚胺过程中，采用有机碱三乙胺作催化剂，同时加入金属铜盐阻聚剂，使N－苯基马来酰亚胺的产率比文献报道用乙酸钠作催化剂时明显提高，达到85％。加入四聚剂后，N－苯基马来酰亚胺的纯度提高到99％以上。
In the course of synthesizing heat-resistant modifer N-phenyl maleimide, aniline and maleic anhydride were used as main materials. When organic base triethylamine was employed as catalyst and metallic copper salt was added as polymerization-retarder simultaneously, the yield of N-phenyl maleimide can reach 85%, which was higher than that using acetic sodium as catalyst.Moreover the purity of N-phenyl maleimide was improved to over 99% when adopting polymerization-retarder.
出处
《山东化工》
CAS
1999年第5期11-13,共3页
Shandong Chemical Industry
关键词
苯基马来酰亚胺
耐热
改性剂
高分子
N-phenyl maleimide
heat-resistant modifer
function macromolecular
