摘要
以３－Ｎ，Ｎ－二甲胺基－１，２－二氯丙烷和Ｏ，Ｏ′－二甲基二硫代磷酸酯合成了一种新杀虫剂Ｏ，Ｏ，Ｏ′，Ｏ′－四甲基－Ｓ，Ｓ′－（２－Ｎ，Ｎ－二甲胺基丙撑）－双－二硫代磷酸酯（沙蚕磷）并制备了它的草酸盐，鉴定了其草酸盐的晶体结构，测试了它们的生物活性。
A new insecticide O,O,O′,O′-tetramethyl-S,S′-(2-N,N-dimethylamino-trimethylene)-bis-dithiophosphate(Shacanlin)was synthesized from 3-N,N-dimethylamino-1,2-dichloropropane and O,O′-dimethylphosphorodithioic acid.The crystal of Shacanlin ethane diacid salt was prepared by recrystallize method.The crystal structure was determined by X-ray diffraction,NMR and MS.Its biological activity was determined at laboratory.
出处
《农药》
CAS
北大核心
1998年第8期10-12,共3页
Agrochemicals
基金
贵州省自然科学基金
关键词
沙蚕磷
合成
生物活性
测试
有机磷杀虫剂
synthesis,crystal structure,LD50,O,O,O′,O′-tetramethyl-S,S′-(2-N,N-dimetylamino-trimethylene)-bis-dithiophosphate.
