摘要
根据纳氏比色法测定氨氯的原理,设计制造了名为“肉类新鲜度快速检测仪”的仪器,应用此自制的仪器,一件肉类样品的检测仅需8min。试验表明,吸光度与NH4^+浓度在0~40mg/100g试样之间呈线性关系,其相关系数大于0.995,其检出限(3S/N)为0.5mg/100g。分析两件NH^+浓度不同的试样,测定结果的平均RSD(n=8)值为3.5%
Based on the principle of the Nessler's eolorimetric determination of NH4^+ ion, a new instrument, named "Rapid Determinator for Meat-freshness" was designed and fabricated. By using this self-made determinator, freshness of a meat sample was determined within 8 min. Linear relationship was obtained between the absorbance and concentration of NH4^+ in the range of 0-40 mg per 100 g of sample, with its correlation coefficient over 0. 995 and detection limit of 2. 5 mg per 100 g (3S/N). The average value of RSD's (n=8) found in the analysis of 2 samples with different concentrations of NH4^+ was 3. 5 %,
出处
《理化检验(化学分册)》
CAS
CSCD
北大核心
2006年第12期1032-1033,1062,共3页
Physical Testing and Chemical Analysis(Part B:Chemical Analysis)
关键词
肉类
新鲜度
纳氏试剂
快速测定仪
Meat
Freshness Nessler's reagent
Rapid determinator