摘要
通过苄基三乙基氯化铵的相转移催化作用,过量的环氧氯丙烷与烯丙醇在氢氧化钠水溶液中反应,合成了烯丙基缩水甘油醚,研究了反应时间、温度、碱用量、催化剂用量及环氧氯丙烷用量对产物收率的影响.
By the phase transfer catalysis of benzyl triethyl ammonium chloride, excessive epichlorohydrin reacted with allyl alcohol in the aqueous solution of sodium hydroxide and synthesized allyl glycidyl ether.The effect of reaction time, temperature,dosage of base,catalyst and epichlorohydrin on product yield are studied.
出处
《山东师范大学学报(自然科学版)》
CAS
1996年第1期53-56,共4页
Journal of Shandong Normal University(Natural Science)
关键词
相转移催化
烯丙基
环氧丙基醚
合成
Allyl glycidyl ether
Allyl alcohol
Epichlorohydrin
Benzyl triethyl ammonium chloride
Phasetransfer
catalysis Etherfication