摘要
以内型异莰烷基甲醛与叔丁胺反应制得亚胺,再依次和溴化乙基镁、碘乙烷反应制得了α-乙基异莰烷基甲醛的亚胺,后者经酸水解得向型α-乙基异莰烷基甲醛.该文还对α-乙基异莰烷基甲醛的亚胺及内型α-乙基异茨烷基甲醛的结构进行了测定与讨论.
This paper describes the synthesis of endo-α-ethyliscamphanylformaldehyde through the acid hydrolysis of α-ethylisocamphaylmethylenimine,whih is derived from the reaction of endo-isocamphanylformaldehyde and t-butylamine.The structures of α-ethylisocamphaylmethylenimine and endo-α-ethylisocamphanylformaldehyde are also identified and discussed.
出处
《江西师范大学学报(自然科学版)》
CAS
1996年第2期156-158,共3页
Journal of Jiangxi Normal University(Natural Science Edition)
基金
江西省自然科学基金