摘要
以三聚氯氰为原料,硫化钠为巯基化试剂,在温度为60～70 ℃,pH=9的条件下,制备了2,4,6-三巯基-1,3,5-三嗪(收率≥90%)及其三钠盐.并对制备的2,4,6-三巯基-1,3,5-三嗪和瑞士Fluka公司相同的产品进行了红外光谱分析.
2,4,6 - trithione - 1,3,5 - triazine and its trisodium salt were synthesized from cyanuric chloride by sulfhylization with sodium sulfide at 60-70℃ ,maintaining the pH=9 by addition of NaOH aqueous solution. The yield of 2,4,6 - trithione - 1,3,5 - triazine is ≥90%, and its structure was identified by IR spectrum and the IR spectrum of 2,4,6 - trithione - 1,3,5 - triazine was consistent with the IR spectrum of Fluka product.
出处
《武汉化工学院学报》
2005年第4期8-10,共3页
Journal of Wuhan Institute of Chemical Technology
