A novel method for analysis of three active components curcumin, demethoxycurcumin and bisdemethoxycurcumin in Curcuma longa L. was developed by HPLC coupled with electrochemical detection. Three curcuminoids were wel...A novel method for analysis of three active components curcumin, demethoxycurcumin and bisdemethoxycurcumin in Curcuma longa L. was developed by HPLC coupled with electrochemical detection. Three curcuminoids were well separated on a C18 column and detected with high sensitivity. A mobile phase containing acetonitrile and 10 mM Na2HPO4-H3PO4 （pH 5.0） （50：50, v/v） was used. Good linearity was obtained in the range of 0.208-41.6, 0.197-39.4, and 0.227-114μM for curcumin, demethoxycurcumin and bisdemethoxycurcumin respectively. The limit of detection reached up to 10 ？ 8 M, which was lower than that by UV detection. The relative standard deviations （RSDs） ranged from 1.06%to 1.88%for intra-day precision and from 4.30%to 5.79%for inter-day precision, respectively. The proposed method has been applied in real herb sample and recoveries ranging from 86.3%to 111%were obtained.展开更多
Target detection for wideband radar has recently received extensive attention. The classical energy integrating(EI)detector will always accumulate excess clutter or noise energy,which leads to unacceptable performance...Target detection for wideband radar has recently received extensive attention. The classical energy integrating(EI)detector will always accumulate excess clutter or noise energy,which leads to unacceptable performance deterioration if the detection window is not selected properly. In this paper, an EI detector for the distributed targets in the Gaussian environment is proposed.First, at the stage of preparatory work, the target models are proposed, then, the problem formulation is introduced. Subsequently,in the aspect of optimizing the method of detection window search and the method of threshold setting, the detailed design stages of the proposed detector are provided. Furthermore, theoretical analyses show that the proposed detector is easy to hardware implementation, and it does not need the prior knowledge about the spatial distribution of the target scattering centers in practical radar detection application. Finally, the performance assessment conducted by Monte Carlo simulations verifies that the proposed detector outperforms the conventional detectors.展开更多
基金supported by the National Scientific Foundation of China (Grant nos.21375101,90817103,and 30973672)Doctroral Fund of Ministry of Education of China (No.20110141110024)Innovation Seed Fund and Translational Medical Research Fund of Wuhan University School of Medicine
文摘A novel method for analysis of three active components curcumin, demethoxycurcumin and bisdemethoxycurcumin in Curcuma longa L. was developed by HPLC coupled with electrochemical detection. Three curcuminoids were well separated on a C18 column and detected with high sensitivity. A mobile phase containing acetonitrile and 10 mM Na2HPO4-H3PO4 （pH 5.0） （50：50, v/v） was used. Good linearity was obtained in the range of 0.208-41.6, 0.197-39.4, and 0.227-114μM for curcumin, demethoxycurcumin and bisdemethoxycurcumin respectively. The limit of detection reached up to 10 ？ 8 M, which was lower than that by UV detection. The relative standard deviations （RSDs） ranged from 1.06%to 1.88%for intra-day precision and from 4.30%to 5.79%for inter-day precision, respectively. The proposed method has been applied in real herb sample and recoveries ranging from 86.3%to 111%were obtained.
基金supported by the National Natural Science Foundation of China(61571043)and the 111 Project of China(B14010)
文摘Target detection for wideband radar has recently received extensive attention. The classical energy integrating(EI)detector will always accumulate excess clutter or noise energy,which leads to unacceptable performance deterioration if the detection window is not selected properly. In this paper, an EI detector for the distributed targets in the Gaussian environment is proposed.First, at the stage of preparatory work, the target models are proposed, then, the problem formulation is introduced. Subsequently,in the aspect of optimizing the method of detection window search and the method of threshold setting, the detailed design stages of the proposed detector are provided. Furthermore, theoretical analyses show that the proposed detector is easy to hardware implementation, and it does not need the prior knowledge about the spatial distribution of the target scattering centers in practical radar detection application. Finally, the performance assessment conducted by Monte Carlo simulations verifies that the proposed detector outperforms the conventional detectors.
