With Nb-Ti-stabilized 430 ferritic stainless steel(NTS430FSS) and SUS 430 ferritic stainless steel(SUS430FSS) as experimental materials, the influence of precipitation on intergranular corrosion resistance was inv...With Nb-Ti-stabilized 430 ferritic stainless steel(NTS430FSS) and SUS 430 ferritic stainless steel(SUS430FSS) as experimental materials, the influence of precipitation on intergranular corrosion resistance was investigated. A series of aging treatment were carried out. The free-exposure corrosion test and double loop electrochemical potentiokinetic reactivation(DL-EPR) test with a scan rate of 1.67 m V/s at 26 °C were applied to evaluate the intergranular corrosion(IGC) resistance. Metallographic observation, scanning electron microscope(SEM), transmission electron microscope(TEM) with energy dispersive spectroscopy(EDS) and X-ray diffraction(XRD) analysis were conducted. The results show that IGC occurred in SUS430 FSS aged above 700 °C, while it occurred in NTS430 FSS as the temperature was improved to 1 050 °C. The critical degree of sensitization Ir/Ia reaches 0.305 in SUS430 FSS, which is higher than that of NTS430 FSS, i.e. 0.010, aged at 950 °C for 2 h. The TEM, EDS and XRD results show that a large amount of Cr23C6 precipitates with size of 60 nm×22 nm are located at the SUS430 FSS grain boundaries as chains. With the addition of Nb and Ti and reduction of C, the amount of precipitates reduces significantly in NTS430 FSS. A majority of Cr23C6 were replaced by Ti C and Nb C. Only a small amount of spherical Ti C(R=186 nm) and square Ti N(312 nm×192 nm) with Nb and Cr adsorbed are left along grain boundaries. Due to the dual stabilization of Nb and Ti, the precipitation of Cr23C6 is restrained, the chromium depleted region is avoided and accordingly the resistance to the intergranular corrosion is improved.展开更多
To address the low accuracy and stability when applying classical control theory in distribution networks with distributed generation,a control method involving flexible multistate switches(FMSs)is proposed in this st...To address the low accuracy and stability when applying classical control theory in distribution networks with distributed generation,a control method involving flexible multistate switches(FMSs)is proposed in this study.This approach is based on an improved double-loop recursive fuzzy neural network(DRFNN)sliding mode,which is intended to stably achieve multiterminal power interaction and adaptive arc suppression for single-phase ground faults.First,an improved DRFNN sliding mode control(SMC)method is proposed to overcome the chattering and transient overshoot inherent in the classical SMC and reduce the reliance on a precise mathematical model of the control system.To improve the robustness of the system,an adaptive parameter-adjustment strategy for the DRFNN is designed,where its dynamic mapping capabilities are leveraged to improve the transient compensation control.Additionally,a quasi-continuous second-order sliding mode controller with a calculus-driven sliding mode surface is developed to improve the current monitoring accuracy and enhance the system stability.The stability of the proposed method and the convergence of the network parameters are verified using the Lyapunov theorem.A simulation model of the three-port FMS with its control system is constructed in MATLAB/Simulink.The simulation result confirms the feasibility and effectiveness of the proposed control strategy based on a comparative analysis.展开更多
文摘With Nb-Ti-stabilized 430 ferritic stainless steel(NTS430FSS) and SUS 430 ferritic stainless steel(SUS430FSS) as experimental materials, the influence of precipitation on intergranular corrosion resistance was investigated. A series of aging treatment were carried out. The free-exposure corrosion test and double loop electrochemical potentiokinetic reactivation(DL-EPR) test with a scan rate of 1.67 m V/s at 26 °C were applied to evaluate the intergranular corrosion(IGC) resistance. Metallographic observation, scanning electron microscope(SEM), transmission electron microscope(TEM) with energy dispersive spectroscopy(EDS) and X-ray diffraction(XRD) analysis were conducted. The results show that IGC occurred in SUS430 FSS aged above 700 °C, while it occurred in NTS430 FSS as the temperature was improved to 1 050 °C. The critical degree of sensitization Ir/Ia reaches 0.305 in SUS430 FSS, which is higher than that of NTS430 FSS, i.e. 0.010, aged at 950 °C for 2 h. The TEM, EDS and XRD results show that a large amount of Cr23C6 precipitates with size of 60 nm×22 nm are located at the SUS430 FSS grain boundaries as chains. With the addition of Nb and Ti and reduction of C, the amount of precipitates reduces significantly in NTS430 FSS. A majority of Cr23C6 were replaced by Ti C and Nb C. Only a small amount of spherical Ti C(R=186 nm) and square Ti N(312 nm×192 nm) with Nb and Cr adsorbed are left along grain boundaries. Due to the dual stabilization of Nb and Ti, the precipitation of Cr23C6 is restrained, the chromium depleted region is avoided and accordingly the resistance to the intergranular corrosion is improved.
基金the Natural Science Foundation of Fujian,China(No.2021J01633).
文摘To address the low accuracy and stability when applying classical control theory in distribution networks with distributed generation,a control method involving flexible multistate switches(FMSs)is proposed in this study.This approach is based on an improved double-loop recursive fuzzy neural network(DRFNN)sliding mode,which is intended to stably achieve multiterminal power interaction and adaptive arc suppression for single-phase ground faults.First,an improved DRFNN sliding mode control(SMC)method is proposed to overcome the chattering and transient overshoot inherent in the classical SMC and reduce the reliance on a precise mathematical model of the control system.To improve the robustness of the system,an adaptive parameter-adjustment strategy for the DRFNN is designed,where its dynamic mapping capabilities are leveraged to improve the transient compensation control.Additionally,a quasi-continuous second-order sliding mode controller with a calculus-driven sliding mode surface is developed to improve the current monitoring accuracy and enhance the system stability.The stability of the proposed method and the convergence of the network parameters are verified using the Lyapunov theorem.A simulation model of the three-port FMS with its control system is constructed in MATLAB/Simulink.The simulation result confirms the feasibility and effectiveness of the proposed control strategy based on a comparative analysis.