The Analects is one of the classic works of the Confucian school,and it is also a treasure house of the wisdom of Chinese nation.While int rodueing the translation of the Analects of Chinese and Mongolian translated b...The Analects is one of the classic works of the Confucian school,and it is also a treasure house of the wisdom of Chinese nation.While int rodueing the translation of the Analects of Chinese and Mongolian translated by M Hatu and T Sod,this artiele summa rizes the characteristics of this translation that distinguish it from other Mongolian versions.展开更多
目的:建立蒙药材木棉花萼的质量标准。方法:对不同产地的蒙药材木棉花萼进行性状鉴别、显微鉴别、薄层色谱鉴别。建立测定木棉花萼中芒果苷含量的HPLC法。色谱柱为Agilent Eclipse Plus C_(18)色谱柱(250 mm×4.6 mm,5μm);以乙腈-1...目的:建立蒙药材木棉花萼的质量标准。方法:对不同产地的蒙药材木棉花萼进行性状鉴别、显微鉴别、薄层色谱鉴别。建立测定木棉花萼中芒果苷含量的HPLC法。色谱柱为Agilent Eclipse Plus C_(18)色谱柱(250 mm×4.6 mm,5μm);以乙腈-1%冰醋酸水溶液(12∶88)为流动相进行梯度洗脱;流速为1.0 m L·min^(-1);检测波长为258 nm;柱温为30℃;进样量为10μL。结果:薄层色谱鉴别中,薄层图谱清晰,与相邻斑点分离较好,阴性对照无干扰;高效液相色谱含量测定中,芒果苷在0.08388μg^0.8388μg范围内呈良好的线性关系。回归方程为:Y=73.853X-0.3706,R^2=0.9999。结论:所建立的显微鉴别、薄层鉴别方法和高效液相含量测定方法简便、可靠、重复性好、专属性强,可作为蒙药材木棉花萼的质量控制方法。展开更多
文摘The Analects is one of the classic works of the Confucian school,and it is also a treasure house of the wisdom of Chinese nation.While int rodueing the translation of the Analects of Chinese and Mongolian translated by M Hatu and T Sod,this artiele summa rizes the characteristics of this translation that distinguish it from other Mongolian versions.
文摘目的:建立蒙药材木棉花萼的质量标准。方法:对不同产地的蒙药材木棉花萼进行性状鉴别、显微鉴别、薄层色谱鉴别。建立测定木棉花萼中芒果苷含量的HPLC法。色谱柱为Agilent Eclipse Plus C_(18)色谱柱(250 mm×4.6 mm,5μm);以乙腈-1%冰醋酸水溶液(12∶88)为流动相进行梯度洗脱;流速为1.0 m L·min^(-1);检测波长为258 nm;柱温为30℃;进样量为10μL。结果:薄层色谱鉴别中,薄层图谱清晰,与相邻斑点分离较好,阴性对照无干扰;高效液相色谱含量测定中,芒果苷在0.08388μg^0.8388μg范围内呈良好的线性关系。回归方程为:Y=73.853X-0.3706,R^2=0.9999。结论:所建立的显微鉴别、薄层鉴别方法和高效液相含量测定方法简便、可靠、重复性好、专属性强,可作为蒙药材木棉花萼的质量控制方法。
