摘要
以钨酸钠为催化剂在微波照射条件下 ,用 3 0 %H2 O2 使 1 ,2 己二醇氧化开环合成己二酸。考察了照射时间、溶液pH值、不同催化剂及催化剂循环使用等对反应的影响 ,找出了反应的最佳条件。
Adipic acid was synthesized from 1,2-cyclohexanediol with 30% H 2O 2 using Na 2WO 4·2H 2O as a catalyst under microwave irradiation. The amounts of catalyst, the irradiation time and different catalysts were investigated and the optimum experimental conditions were found.
出处
《合成化学》
CAS
CSCD
2004年第1期9-11,共3页
Chinese Journal of Synthetic Chemistry
基金
theNationalNaturalScienceFoundationofChina( 2 0 1 72 0 3 9)
