摘要
以三氯硅烷与 3—氯丙烯为原料在氯铂酸复合催化剂催化下合成了 3—氯丙基三氯硅烷 ,继而用甲醇醇解 ,合成了 3—氯丙基三甲氧基硅烷 ,总收率 80 %.
In this paper,the methodes of preporation of 3-chloropropyltrimethoxysilane were discussed.By using complex catalyst contained chloroplatinic acid,trichlorosilane reacted with allyl chloride to give 3-Chloropropyltrichlorosilane in 85% yield.3-Chloropropyltrimethoxysilane was prepared through methoxylotion of the formed 3-Chloropropyltrichlorosilane by dropping simultaneusly anhydrons methanol and the chlorosilane to boilling petroleum ether,in 95% yield.
出处
《河南教育学院学报（自然科学版）》
2002年第2期31-32,共2页
Journal of Henan Institute of Education(Natural Science Edition)
