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某氰化尾渣预氧化——蓄热还原同步提铁试验研究 被引量:2

Experiment Study on Synchronous Iron Extraction of Pre-oxidation and Heat-retaining Reduction for a Cyanide Tailings
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摘要 辽宁新都黄金选金焙烧氰化尾渣总氰含量719 mg/kg,尾渣中铁矿物主要以赤铁矿的形式存在,TFe品位为35.08%。采用预氧化—蓄热还原同步提铁技术处理氰化尾渣,可实现在氰化物高效分解的同时回收铁精矿。研究结果表明,将氰化尾渣样品预先在550℃的空气气氛下焙烧25 min,可将氰化尾渣中的总氰含量降至检出限以下,同时完成对氰化尾渣的蓄热。将预氧化处理后的尾渣在还原温度560℃、还原时间30 min、CO浓度40%、总气量500 mL/min的条件下进行蓄热还原试验。焙烧产品使用棒磨机磨至-0.038 mm占82.02%,后在磁场强度143.28 kA/m条件下进行弱磁选,最终得到TFe品位58.94%,回收率89.93%的铁精矿。该工艺不仅将氰化物有效分解,还实现了氰化尾渣中铁矿物的高效回收利用。 The total cyanide contents of a gold-selecting roasting cyanide tailings from Liaoning Xindu Gold is 719 mg/kg.The main iron minerals in residue is mainly hematite and the TFe grade is of 35.08%.The iron concentrate could be recycled from the cyanide tailings with the decomposition of cyanide efficiently by synchronous iron extraction of per-oxidation and heat-retaining reduction.The results showed that the total cyanide content in cyanide tailings can be reduced to below the detection limit at 550℃,25 min in the cyanide-oxidation stage,and the heating of the tailings was completed.Then,under the condition of reduction temperature of 560℃,reduction time of 30 min,CO concentration of 40%,gas flow of 500 mL/min,the heat-retaining reduction tests was carried out.The iron concentrate with a TFe grade of 58.94%and the recovery of 89.93%was obtained by low intensity magnetic separation at magnetic field intensity of 143.28 kA/m after being ground to-0.038 mm accounting for 82.02%by rod mill.This process can not only oxidize the cyanide effectively,but also realize efficient recovery and utilization of iron minerals from cyanide tailing.
作者 赵羚伯 赵冰 高鹏 董再蒸 ZHAO Lingbo;ZHAO Bing;GAO Peng;DONG Zaizheng(School of Resources and Civil Engineering,Northeastern University,Shenyang 110819,China;National-local Joint Engineering Research Center of High-efficient Exploitation Technology for Refractory Iron Ore Resources,Shenyang 110819,China;State Key Laboratory of Rolling and Automation,Northeastern University,Shenyang 110819,China)
出处 《金属矿山》 CAS 北大核心 2022年第7期170-174,共5页 Metal Mine
基金 国家自然科学基金项目(编号:52004056) 辽宁省“兴辽英才计划”项目(编号:XLYC1908017,XLYC1907162) 中央高校基本科研业务费专项(编号:N2130001)。
关键词 氰化尾渣 蓄热还原 磁化焙烧 磁选 cyanide tailings heat-retaining reduction magnetizing roasting magnetic separation
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