摘要
利用顶空固相微萃取(HS-SPME)结合气质联用(GC-MS)技术对桂枝茯苓丸、桂枝茯苓片、桂枝茯苓胶囊3种不同剂型的挥发性成分进行了分析,并且计算了各成分相对百分含量。结果表明,从桂枝茯苓丸中检测出22个峰,鉴定出17种成分,占挥发性成分的98.41%;从桂枝茯苓片中检测出15个峰,鉴定出12种成分,占挥发性成分的89.12%;从桂枝茯苓胶囊中检测出30个峰,鉴定出26种成分,占挥发性成分的99.46%。桂枝茯苓丸及其他剂型之间挥发性成分的组成和含量均发生了变化。
Headspace solid phase microextraction(HS-SPME)combined with gas chromatography-mass spectrometry(GC-MS)was used to analyze the volatile components of Guizhi Fuling bolus,Guizhi Fuling tablets and Guizhi Fuling capsules,the relative contents of each component were calculated. The results showed that 22 peaks were detected from Guizhi Fuling bolus,17 components were identified,accounting for 98.41% of the volatile components,15 peaks were detected from Guizhi Fuling tablets,12 components were identified,accounting for 89.12% of the volatile components,and 30 peaks were identified from Guizhi Fuling capsules,accounting for 99.46% of the volatile components. The composition and content of volatile components in Guizhi Fuling bolus and other dosage forms changed.
作者
马银宇
卢金清
罗贝贝
MA Yin-yu;LU Jin-qing;LUO Bei-bei(Hubei University of Chinese Medicine/Research and Development Center of Medicinal Plant in Hubei Province,Wuhan 430065,China)
出处
《湖北农业科学》
2020年第9期155-158,共4页
Hubei Agricultural Sciences
基金
湖北省技术创新专项重大项目(2016ACA146)。