摘要
以乙炔和 1 ,4-丁二醇作为原料 ,在常温常压下合成了羟丁基乙烯基醚 ,并进行了分离与提纯。同时对产物用红外光谱 ,紫外光谱与元素分析进行了表征。讨论了引发剂、氧气、精制前预处理。
Acetylene reacted with butanediol to give vinyl 4 hydroxybutyl ether at ambient temperature and pressure. The product was purified and characterized by gas chromatography, ultraviolet spectroscopy, infrared spectroscopy and elemental analysis. The effect of initiator、oxygen、purification method and equipment on conversion and purity of vinyl 4 hydroxybutyl ether was discussed.
出处
《化学世界》
CAS
CSCD
北大核心
2002年第10期540-543,532,共5页
Chemical World
关键词
羟丁基乙烯基醚
精制
合成
乙炔
1
4-丁二醇
vinyl 4 hydroxybutyl ether
purification
synthesis at ambient temperature and pressure
