摘要
以1H-1,2,4-三唑和3-(2,4-二氯苯基)丙酸为起始原料,经过缩合、氯化和酯化等反应,合成了标题化合物3-(2,4-二氯苯基)丙酸1H-1,2,4-三唑基甲醇酯。用甲醇作为溶剂重结晶,得到了标题化合物的单晶,并且通过IR、1H NMR和X-射线衍射等方法确证了其结构。
（1H-1,2,4-Triazol-l-yl） methyl 3-（2,4-dichlorophenyl） propanoate has been synthesized from 1H-1,2,4-triazol and 3-（2,4-dichlorophenyl） propanoic acid, through condensation, chlorination and esterification reaction. The single crystal of the title compound has been obtained by recrystallization with methanol as solvent. Its structure has been confirmed through diffractions oflR, IH NMR and X-ray, etc.
出处
《洛阳理工学院学报（自然科学版）》
2014年第2期5-9,共5页
Journal of Luoyang Institute of Science and Technology：Natural Science Edition
关键词
1H-1
2
4-三唑基甲醇酯
制备
结构表征
（1H-1,2,4-triazol-l-yl） methyl ester
preparation
structural characterization
