摘要
报道了标题化合物的合成,其结构经X-射线衍射分析得到了表征。化合物为单斜晶系,P21/c空间群,相关晶体数据为:a=1.3420(3)nm,b=0.9720(2)nm,c=0.7900(2)nm,β=92.00(3)°,V=1.0299(4)nm3,Z=4,Dc=1.429g/cm3,F(000)=456,μ=0.345nm-1,R=0.0435,wR=0.0894。晶体分子通过氢键以及分子间作用力相互连接在一起,形成超分子键,并通过氢键相互连接,形成三维网状结构,使分子结构更加趋于稳定。
The title compound was synthesized and characterized by IR and X-ray crystallography. The crystal belongs to monoclinic, P2 1/c grou, with crystal data: a=1.342 0(3) nm ,b=0.972 0(2) nm, c=0,790 0(2) nm, β=92.00(3)°, V=1.029 9(4) nm^3, Z=4,D c=1.429 g/cm^3,F(000)=456,μ=0.345 nm^(-1),R=0.043 5,wR=0.089 4.There exists intermolecular hydrogen bond in the crystal,which forms three-dimensional network and makes the crystal more stable.
出处
《承德石油高等专科学校学报》
CAS
2004年第4期14-17,22,共5页
Journal of Chengde Petroleum College
