摘要
在对甲基苯磺酸的催化下 ,利用微波技术 ,快速合成了肉桂酸异戊酯。最佳反应条件为 :异戊醇和肉桂酸的摩尔比为 1 5 :1(mol/mol) ,催化剂 0 30g ,微波功率 5 95W ,微波辐射时间 6min ,转化率 93 2 %
Isoamyl cinnamate is syntheticed fastly with the techinigue of microwave,under the condition of catalyzing methylbenzene sutfonic acid the best reaction conditions are the mole ratio of isoamyl alcohol and cinnamic acid is 2:1(mol/mol),the amount of catalyst is 0.30g,the power of miorwave is 595W,the radiating time of microwave is 6 min,the transformingpercentage may reach 93.2%.
出处
《化学工程师》
CAS
2002年第2期5-6,共2页
Chemical Engineer