摘要
利用微波辐射 ,以FeCl3 ·6H2 O为催化剂 ,使 2 -萘酚进行氧化偶联反应 ,合成外消旋 1,1′ -联- 2 -萘酚 ,反应时间 2min ,产品产率 98.5 % ,m .p .2 15～ 2 16℃ .
Racemic 1,1′ -bi-2-naphthol were synthesized by oxidation-coupled reaction when the naphthol with FeCl 3·6H 2O as catalyst were subjected to microwave irradiation. The reaction timeis 2 min. m.p. 215～216 ℃. The yield is 98.5%.
出处
《河北大学学报（自然科学版）》
CAS
2001年第4期389-390,共2页
Journal of Hebei University(Natural Science Edition)
