摘要
利用微波辐射以FeCl3为催化剂,使2-萘酚进行氧化偶联反应,合成外消旋β,β′—联萘酚,反应时间为3min,产品产率为39.8%,熔点为216~217℃.
Racemic β,β′-bi naphthol were synthesized by oxidation-coupled reaction when the naphthol with as catalyst were subject to microwave irradiation.The reaction times 3 min.m.p.216~217 ℃.The yield is 39.8%.
出处
《吉林师范大学学报(自然科学版)》
2005年第1期52-53,共2页
Journal of Jilin Normal University:Natural Science Edition