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复凝聚法制备2,5-二苯基噻吩微胶囊剂 被引量:6

Preparation of 2,5-diphenylthiophene microcapsule by complex coacervation method
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摘要 以光活化杀虫剂2,5-二苯基噻吩为芯材,明胶、阿拉伯胶为壁材,采用复凝聚法制备2,5-二苯基噻吩微胶囊剂,研究并确定了微胶囊化的最佳工艺条件.结果表明:明胶、阿拉伯胶水溶液复凝聚反应时,控制pH=4.2,温度为45℃,搅拌速度为1 500r·min-1的条件,混合搅拌20min所制备的微胶囊药效最佳,平均粒径为4.92μm,包封率可达70.53%. Abstract: 2,5- Diphenylthiophene microcapsule was prepared with gelatin and arabic gum as wall materials and 2,5 - diphenylthiophene as microcapsule core by complex coacervation method. The optimal preparation process condition was obtained by the experiment. The results indicate the opti- mal preparation process condition is: reaction temperature being 45 ℃, pH being 4.2, time for complex coacervation method being 20 rain and stirring revolutions being 1 500 r ·min-1. Uniform spherical microcapsules are thus obtained with an average particle size of 4.92μm. The encapsula- tion efficiency is up to 70.53 %.
出处 《扬州大学学报(自然科学版)》 CAS 北大核心 2014年第1期30-33,共4页 Journal of Yangzhou University:Natural Science Edition
基金 江苏省科技支撑计划项目(BE2012364) 全国大学生实践创新训练计划项目(20121117039) 江苏省大学生实践创新训练计划资助项目(2012JSSPITP1351) 扬州大学科技创新培育基金(2012CXJ065)
关键词 复凝聚法 2 5-二苯基噻吩 微胶囊剂 complex coacervation method, 2,5 - diphenylthiophene~ microcapsule
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