摘要
以糠醛和氨基硫脲为原料,冰醋酸为催化剂,制备了希夫碱,用该希夫碱与醋酸铜合成了配合物,用红外光谱和紫外光谱对其结构进行了表征。同时测定了希夫碱及配合物熔点、测试其溶解性,讨论了影响希夫碱产率的因素。
Furaldehyde-thiosemicarbazide was synthesized from furaldehyde and thiosemicarbazide with HAc as catalyst, and then its copper complex was synthesized. The melting points of the compounds were determined and their solubility was tested. Their structures were characterized by UV and IR spectroscopy. The factors influencing the yield were discussed.
出处
《化学世界》
CAS
CSCD
北大核心
2013年第9期554-556,共3页
Chemical World
关键词
糠醛
氨基硫脲
希夫碱
金属配合物
furaldehyde
thiosemicarbazide
Schiff base
metal complex
