摘要
用电化学金属阳极氧化法在非水溶剂中合成了苯乙酮双缩硫代对称二氨基脲 (HL)与Cu(Ⅰ ) ,Zn(Ⅱ ) ,Fe(Ⅱ )的配合物 ,通过元素分析、红外光谱、紫外光谱、磁化率、摩尔电导等对配合物进行了表征 .
Cu(I), Zn(II), Fe(II) complexes of 1,5 bis(acetophenone) thiocarbohydrazone were synthesized by the electrochemical oxidation of anodic metal in non aqueous solution. The complexes were characterized by elemental analysis, IR, UV, magnetic measurement and molar conductivity.
出处
《宁夏大学学报(自然科学版)》
CAS
2000年第3期244-246,共3页
Journal of Ningxia University(Natural Science Edition)
基金
甘肃省自然科学基金资助项目!(95 0 5 )
关键词
电化学
合成
金属有机化合物
含硫希夫碱
electrochemical synthesis
1
5 bis(acetophenone) thiocarbohydrazone
metal organic compound