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Low polar volatile constituents from Isodon excisa by GC-MS 被引量:1

Low polar volatile constituents from Isodon excisa by GC-MS
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摘要 An attempt had been made to isolate and identify the low polar volatile constituents from Isodon excisa. The dried plants were heat extracted with ethanol and then extracted with petroleum ether. The constituents were isolated and analyzed by GC-MS and then we retrieved them on NIST08 mass spectrometry database to determine their structures. Finally, successful results were achieved, 111 compounds were obtained and identified. 105 of them were reported for the first time in lsodon excisa and 22 of them were first found in natural products. Thus, the main constituents of it were found to be Sitosterol (33.28%), 3-Amino-4-pyrazolecarbonitrile (9.55%) An attempt had been made to isolate and identify the low polar volatile constituents from Isodon excisa. The dried plants were heat extracted with ethanol and then extracted with petroleum ether. The constituents were isolated and analyzed by GC-MS and then we retrieved them on NIST08 mass spectrometry database to determine their structures. Finally, successful results were achieved, 111 compounds were obtained and identified. 105 of them were reported for the first time in Isodon excisa and 22 of them were first found in natural products. Thus, the main constituents of it were found to be Sitosterol (33.28%), 3-Amino-4-pyrazolecarbonitrile (9.55%).
机构地区 School of Pharmacy
出处 《Journal of Medical Colleges of PLA(China)》 CAS 2012年第6期334-342,共9页 中国人民解放军军医大学学报(英文版)
关键词 lsodon excise Petroleum ether GC-MS Low polar volatile compounds GC-MS分析 挥发性成分 香茶菜 极性 石油醚萃取 质谱数据库 乙醇萃取 天然产物
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