摘要
目的:研究山风乙酸乙酯萃取部位的化学成分。方法:采用柱色谱分离技术,从壮药山风全草的80%乙醇提取物的乙酸乙酯萃取部位中分离到7个化合物,并使用MS和NMR分析,鉴定化合物结构。结果:分得7个化合物,分别鉴别为:花椒素(1)、邻苯二甲酸二丁酯(2)、β-谷甾醇(3)、甲基异茜草素(4)、圣草酚(5)、山柰酚(6)、7,3'-O-二甲基芦丁(7)。结论:以上化合物均为从该植物中首次分离得到。其中,化合物2、4、7为从该属植物中首次分离。
Objective:To study the chemical constituents of the ethyl acetate extract from Blumea aromatica.Methods:Column chromatographic techniques were used for the isolation and purification.Spectroscopic techniques were used for the identification of structures.Results:Seven compounds were isolated from the ethyl acetate extract of 80% alcohol extract of the whole plant,and their structures were identified as xanthoxylin(1),dibutyl phthalate(2),luteolin-3′,4′,7-trimethyl ether(3),rubiadin(4),eriodictyol(5),kaempherol(6),luteolin 7,3′-dimethyl ether(7).Conclusion:All the compounds are isolated from this plant for the first time.Among them,compounds 2,4 and 7 are isolated from this genus for the first time.
出处
《中药材》
CAS
CSCD
北大核心
2012年第2期229-231,共3页
Journal of Chinese Medicinal Materials
关键词
山风
菊科
化学成分
Blumea aromatica(Wall.) DC.
Compositae
Chemical constituents