摘要
以松节油为原料,经水合萜二醇合成了含醇量较高的调香松油醇,根据水合、脱水反应的碳架Wagner-Mectwein重排的原理,研究反应中影响得率的产要因素,并进行正交试验,确定了水合、脱水反应的最佳工艺。
Perfumery terpineol with high alcohol content was synthesized through terpine hydrate from tur-pentine. Main factor afecting the yield in the process of hydration and dehydration reacrions were studied ac-cording to the theory of carbon frame rearrangement by WAGNERD MECRWEIN. As a result, the mostfavourable reaction conditions were determined and cunfirmed.
出处
《林产化学与工业》
EI
CAS
CSCD
北大核心
1994年第S1期135-139,共5页
Chemistry and Industry of Forest Products
关键词
水合萜二醇
松油醇
水合反应
脱水反应
分馏
Terpine hydrate
Terpeneol
Hydration
Dehydration
Fractional distillation