摘要
Using N-bromosuccinimide and pyridine as the oxidation system to dehydrogenate aryl substituted semicarbazide to form azo compounds is described for the first time in this paper. Nine azo compounds have been prepared in excellent yield under mild condition. This method only. needs simple instrument and short reaction time.
Using N-bromosuccinimide and pyridine as the oxidation system to dehydrogenate aryl substituted semicarbazide to form azo compounds is described for the first time in this paper. Nine azo compounds have been prepared in excellent yield under mild condition. This method only. needs simple instrument and short reaction time.
