摘要
目的:建立血府逐瘀丸的质量标准。方法:采用薄层色谱法对血府逐瘀丸中当归、川芎、地黄、红花进行了定性鉴别;采用高效液相色谱法对桃仁中苦杏仁苷的含量进行了测定。结果:薄层色谱斑点清晰,阴性对照无干扰。苦杏仁苷进样量在0.348～3.482μg范围内线性关系良好(r=0.999 9)。平均加样回收率为98.9%,RSD=0.9%(n=6)。结论:该法准确,灵敏,重复性好,可有效控制该制剂的质量。
Objective： To establish the quality standard for Xuefu Zhuyu pills. Method： Angelicae Sinensis Radix, Chuanxiong Rhizoma, Rehmanniae Radix and Carthami Flos were identified by TLC. The content of amygdalin in Xuefu Zhuyu pills was determined by HPLC. Result： The spots on TLC plates were clear without interference. The linear range of amygdalin was 0. 348-3. 482 p,g, r = 0. 999 9. The average recovery of amygdalin was 98.9% （ n = 6） with RSD of 0. 9%. Conclusion： The method is accurate with good reproducibility and specificity. It is suitable for the quality control of Xuefu Zhuyu pills.
出处
《中国药师》
CAS
2011年第5期646-647,共2页
China Pharmacist
