摘要
文章以五溴甲苯为原料,经苄位溴化反应首先得到中间体五溴苄基溴,然后进一步与丙烯酸钠反应得到了丙烯酸五溴苄酯,探讨了溶剂及n(AA):n(PBB-Br)对丙烯酸五溴苄酯合成的影响。并采用IR和1HNMR对产物进行了表征。
In the present work,flame retardent pentabromobenzyl acrylate was synthesized in two steps.Raw material pentabromotoluene was firstly brominated to prepare pentabromobenzyl bromide,which then further reacted with sodium acrylate to obtain the target product.The influences of solvent and n（AA）：n（PBB-Br） on this reaction were investigated.The strcture were characterized by FT-IR and 1H NMR.
出处
《盐业与化工》
CAS
2011年第3期6-7,14,共3页
Jounral of Salt and Chemical Industry
关键词
阻燃剂
五溴苄基溴
丙烯酸五溴苄酯
合成
flame retardent
pentabromobenzyl bromide
pentabromobenzyl acrylate
synthesis
