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无机化学实验教学中对三草酸合铁(Ⅲ) 酸钾制备的实验改进 被引量:8

Optimization of conditions for the preparation of potassium ferrioxalate in teaching and research of inorganic chemistry experiment
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摘要 本文对三草酸合铁(Ⅲ)酸钾的制备实验进行了优化,通过改变剩余H2O2去除时间、酸溶温度、结晶方式得到了结晶粒度较大、晶型均匀、色泽鲜艳的翠绿色菱形晶体,并且产品的产率可达65%。这一实验的改进,有助于激发学生实验兴趣,增进学生实验能力。 The experiment conditions were optimized for the preparation of potassium ferrioxalate. The big emerald crystal was obtained、yield was up to 65% by improving time of elimination H2O2、the temperature of adding H2C2O4、the manner of crystallization.
出处 《教育文化论坛》 2011年第1期90-92,共3页 Tribune of Education Culture
关键词 硫酸亚铁铵 三草酸合铁(Ⅲ)酸钾 制备 优化 ammonium ferrous sulfate potassium ferrioxalate preparation optimization
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