摘要
由四甲基秋兰姆(TMTD)经氯化、硒代与溴代丙酰呋喃(噻吩) 反应,制得了2 种二硒代氨基甲酸酯通过元素分析、红外光谱、核磁共振谱确定了它们的结构,并对反应条件、反应机理做了简略的讨论.
The 1-(2-thienyl-acyl)ethyl-(N,N-dimethyl)diselenocarbamate and 1-(2-furyl-acyl)ethyl-(N,N-dimethyl)diselenocarbamate were synthesized in four steps,the structures of the compounds have been characterized by elemental analysis,IR, 1H NMR.A suitable mechanism about the formation of title compounds were discussed.
出处
《东北师大学报(自然科学版)》
CAS
CSCD
1999年第3期42-45,共4页
Journal of Northeast Normal University(Natural Science Edition)