摘要
本文报道了一种11(S)-药喇叭酸甲酯的合成方法,以商业可得的(R)-缩水甘油为原料,经八步反应,以12%的总收率得到产物。经测定,所合成化合物的1H NMR 1、3C
Thie synthesis of methyl 11(S)-jalapinolate which required 8 steps overall and whose total yield was 12% from(R)-glycidol was reported in this paper.The synthetic methyl 11(S)-jalapinolate was found to be identical with the compound reported in the literatures on the basis of 1H NMR,13C NMR spectra and specific rotation comparisons.
出处
《化学研究与应用》
CAS
CSCD
北大核心
2011年第2期248-251,共4页
Chemical Research and Application