摘要
用Bunte Salt法,以1,2-二氯乙烷和一系列的醛(酮)为原料,乙醇为溶剂,合成了5个环戊烷硫醚类香料(a~e),结果表明,该方法具有操作简单,产率高,环境污染小等优点。用IR,1HNMR和MS证实了目标化合物结构。
Five derivatives of 1,3-Dithiocyclopentane(a- e) were prepared in solvent ethanol, with Bunte Salt, 1,2-dichloroethane and aldehydes or ketones as raw materials, The procedure has the feature of easier operation, higher yield and environmental compatibility, structure of the products was characterized by IR,^1H NMR and MS.
出处
《中国调味品》
CAS
北大核心
2010年第4期115-116,共2页
China Condiment
基金
湖北省高等学校优秀中青年科技创新团队计划资助项目(T200707)