摘要
以对甲苯磺酸为催化剂,乙硫醇和一系列的醛为原料,二氯甲烷为溶剂,合成了一系列新型缩硫醛化合物(a~f),用IR,1HNMR和MS证实了目标化合物的结构,并对一系列目标化合物进行了香气鉴定,结果表明所有目标化合物都具有浓郁的特征气味。
a series of ethylmercaptal(a-f)was prepared in dichloromethane, ethylthiol and a series of aldehyde as raw materials, using p-toluenesulfonic acid as catalyst, the structure of the products was characterized by IR,^1 H NMR and MS. The odour of the product was identified, the result shows that compounds have intense flavor.
出处
《中国调味品》
CAS
北大核心
2009年第8期99-100,共2页
China Condiment
基金
湖北省高等学校优秀中青年科技创新团队计划资助项目(T200707)
关键词
乙硫醇
合成
香气
ethylthiol
synthesis
flavor