摘要
０１ｍｏｌ柠檬醛和过量甲硫醇在１２ｍｍｏｌ无水氯化锌催化下发生反应，合成了相应的缩硫醛，产率７４８％。并通过红外光谱、元素分析、核磁共振检测对产物结构进行了确证。
Citral(0.1mol)was treated with methanethiol in cyclohexane in the presence of anhydrous zinc chloride(12mmol)to give 74.8% citral methane mercaptal.The structure of the product was proved by way of IR spectrum,elementary analysis,1H NMR spectrum datum.
出处
《精细化工》
EI
CAS
CSCD
北大核心
1998年第2期25-26,共2页
Fine Chemicals
