摘要
合成了标题化合物。通过IR1、HNMR及X-射线单晶衍射对其结构进行了表征。该晶体属三斜晶系,P-1空间群,a=11.068(4)nm,b=11.226(5)nm,c=11.916(5)nm,α=83.004(7)°,β=75.641(7),°V=1.337 8(9)nm3,Z=2,Dc=1.094 g/cm3,F(000)=480,R1=0.064 3,wR2=0.200 4。
The title compound had been synthesized and characterized by IR,1HNMR and single-crystal X-ray diffractometry.The test results showed that the crystal belonged to a triclinic system and the P1 space group with following parameters:a=11.068(4) nm,b=11.226(5) nm,c=11.916(5) nm,and α=83.004(7)°,β=75.641(7)°,V=1.337 8(9) nm3,Z=2,Dc=1.094 g/cm3,F(000)=480,R1=0.064 3,and wR2=0.200 4.
出处
《化学试剂》
CAS
CSCD
北大核心
2010年第3期271-272,共2页
Chemical Reagents