摘要
建立了固相萃取结合高效液相法测定地下水中的15种多环芳烃。采用CLEAN—UP C18固相萃取小柱富集水样，系统考察了样品的流速和洗脱剂的强度、用量、有机改性剂加入的量以及氮气浓缩条件对测定的影响。15种多环芳烃的方法检出限为1～146g／L，加标回收率在73．4％～105％之间。本实验方法简便快速、稳定可靠，适用于地下水中15种多环芳烃的测定。
A method of solid-phase extraction and high performance liquid chromatography determination of fifteen polycyclic aromatic hydrocarbons in groundwater has been established, polycyclic aromatic hydrocarbons were extracted from groundwater with CLEAN-UP C,s SPE cartridge, and Various parameters on the determination were studied. （i. e. the sample flow rates, eluent strength, eluent volume, organic modifier concentration and concentrated condition with Nitrogen Evaporators. ） The detection limits were 1 - 14ng· L^-1, and average recoveries 73.4% - 104%. The method is accurate, simple, rapid, stable and reliable, which can be used to determine polycyclic aromatic hydrocarbons in groundwater.
出处
《中国环境监测》
CAS
CSCD
北大核心
2009年第4期19-22,共4页
Environmental Monitoring in China
基金
中国地质调查局地质调查项目(1212010634505)
关键词
固相萃取
高效液相色谱法
多环芳烃
Solid-phase extraction
High-performance liquid chromatography
Polycyelie aromatic hydrocarbons
