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通过格氏反应制备羧酸烷基芴的方法研究 被引量：1

The research on preparation of alkyl fluorenecarboxylic acid by Grignard reaction
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摘要 以9,9-二己基-2,7-二溴代芴和干冰为原料,无水四氢呋喃为溶剂,在一定条件下通过格氏反应制备了2,7-二羧酸-9,9-二己基芴,收率58%。探讨了反应原料、引发剂、溶剂等方面因素对反应的影响。 9,9-dihexyl-fluorene-2,7-dicarboxylic acid was prepared from 2,7-dibromo-9,9- dihexyl fluorene by Gri gnard reaction under appropriate conditions. The yield reached 58%. Some factors affecting the reaction were studied.
作者 赵玮 孙岳明 祁争健 王华林
机构地区 南京信息职业技术学院 南京东南大学化学化工学院
出处 《化工新型材料》 CAS CSCD 北大核心 2009年第1期52-53,共2页 New Chemical Materials
关键词 格氏反应 芴 干冰 Grignard reaction, fluorene,dry ice
分类号 O625.153 [理学—有机化学]
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参考文献9

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共引文献19

同被引文献14

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化工新型材料
2009年 第1期

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