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Silica supported perchloric acid(HClO_4-SiO_2):A mild,reusable and highly efficient heterogeneous catalyst for the synthesis of amidoalkyl naphthols 被引量:7

Silica supported perchloric acid(HClO_4-SiO_2):A mild,reusable and highly efficient heterogeneous catalyst for the synthesis of amidoalkyl naphthols
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摘要 An efficient and direct procedure has been developed for the preparation of amidoalkyl naphthols by a one-pot condensation of aryl aldehydes, 2-naphthol and urea or amides, in the presence of HClO4-SiO2 as a heterogeneous catalyst. The reactions were carried out under reflux and solvent-free conditions. The present methodology offers several advantages such as excellent yields, simple procedure, easy work-up and ecofriendly reaction condition. The catalyst is easily prepared, stable, reusable and efficient under the reaction conditions. An efficient and direct procedure has been developed for the preparation of amidoalkyl naphthols by a one-pot condensation of aryl aldehydes, 2-naphthol and urea or amides, in the presence of HClO4-SiO2 as a heterogeneous catalyst. The reactions were carried out under reflux and solvent-free conditions. The present methodology offers several advantages such as excellent yields, simple procedure, easy work-up and ecofriendly reaction condition. The catalyst is easily prepared, stable, reusable and efficient under the reaction conditions.
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2008年第10期1171-1174,共4页 中国化学快报(英文版)
关键词 ONE-POT HClO4-SiO2 Heterogeneous catalyst Amidoalkyl naphthol Multicomponent reaction One-pot HClO4-SiO2 Heterogeneous catalyst Amidoalkyl naphthol Multicomponent reaction
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