摘要
本文研究建立了食品中姜黄素的高效液相色谱测定方法。样品中的姜黄素经乙醇:氨水(3:1)提取后,聚酰胺吸附,再经甲醇氨水洗脱、浓缩,液相色谱二级管阵列检测器检测。姜黄素标准在0.5μg/mL～50μg/mL范围内具有良好的线性,该方法回收率高,样品定量检测限(LOQ)为0.2mg/kg,可作为糖果、糕点、面制品等食品的定量检测方法。
The determination of ctLrcumin in food by high performance liquid chromatography with photodiode - array detection has been studied. The procedure consists of extraction of sample with ethanol -ammonia（3：1 ）, adsorption with polyamide,elution with basic methanol then concentration. The standard curve was in the range of 0. 5μg/mL^-1 to 50 μg/ mL^-1. Good recoveries were obtained for all analytes and the detection limits were 0.2mg/kg^-1. This method Was suitable for food（ candy, pastry, noodle） as quantitative method.
出处
《福建分析测试》
CAS
2008年第3期28-30,共3页
Fujian Analysis & Testing
基金
厦门市科技计划项目<食品中多种合成着色剂及天然着色剂的快速测定>(项目编号:3502Z20072013)
