摘要
通过皂化的方法将30%的粗品茄尼醇提纯,对粗品茄尼醇的皂化条件进行了研究,探索了皂化温度、皂化时间、NaOH用量和乙醇用量的影响,实验结果用高效液相色谱分析,并用最小方差法关联.结果表明在45℃时,5.0 g粗品茄尼醇中加入2.5 g NaOH和30 ml乙醇,搅拌皂化3小时,能将茄尼醇的含量提高到41.90%.实验和关联值为进一步提纯茄尼醇提供了有效依据.
Saponification was used to refining solanesol from crude solanesol （30%） in this work. The saponification conditions such as saponification temperature, saponification time, amount of NaOH and amount of C2H5OH were studied; these results were analyzed by HPLC and showed the content of solanesol arrived to 41.90% at the optimal conditions, with the saponification time of 3 hours, temperature about 45℃, amount of 2.5 g NaOH and amount of 30 ml C2H5OH for 5.0 g crude solanesol. The Minimum Variance method was applied to correlate the results. The experimental and correlative results provide an effective basis for further research of refining solanesol.
出处
《计算机与应用化学》
CAS
CSCD
北大核心
2008年第6期682-684,共3页
Computers and Applied Chemistry
基金
Supported by Patented Technology for Industrialization Item of Nanjing(07sd156049)
关键词
茄尼醇
皂化
实验和关联
solanesol, saponification, experiment and correlation
