摘要
通过将温度探头伸入高压腔内在线测定了3种传压介质(癸二酸二辛酯、水、无水乙醇)的温度变化情况,研究它们在不同条件下的压致升温规律.结果表明:在试验条件下,癸二酸二辛酯的压致升温值随压力的增加由0.089℃/MPa降至0.068℃/MPa,且随初始温度的增加而降低;水的压致升温值随压力的增加基本不变,稳定在0.026-0.028℃/MPa之间,且随初始温度的增加而略有增加;无水乙醇的压致升温值受压力影响大于水而小于癸二酸二辛酯,随压力增加由0.082℃/MPa降至0.075℃/MPa,初始温度对其影响大于水,但乙醇压致升温值随着其质量分数的增加而增加.通过聚四氟乙烯套筒和不锈钢套筒模拟不同的热损失条件时,在保压过程中前者对癸二酸二辛酯的保温效果明显高于后者.
The compression heating characteristics of three pressure-transmitting fluids such as dioctyl sebacate, water and ethanol in high hydrostatic pressure processing were investigated via the on-line measurement of temperature by inserting the probe into the high-pressure cavity. The results show that ( 1 ) the compression heating value of dioctyl sebacate decreases from 0. 089 to 0. 068 ℃/MPa with the increase in pressure, while that of water slightly changes from 0. 026 to 0. 028℃/MPa, and that of ethanol decreases from 0. 082 to 0. 075℃/100 MPa; ( 2 ) the influence of pressure on the compression heating value of ethanol is greater than that on water but slightly smaller than dioctyl sebacate; (3) with the increase in the initial temperature, the compression heating value of dioctyl sebacate decreases, while that of water slightly increases; (4) the effect of the initial temperature on the compression heating value of ethanol is greater than that of water, which increases with the mass fraction; and (5) teflon liner has greater heat preservation effect on dioctyl sebacate than stainless steel liner during the pressure-holding process in different simulated heat loss conditions.
出处
《华南理工大学学报(自然科学版)》
EI
CAS
CSCD
北大核心
2007年第12期132-136,共5页
Journal of South China University of Technology(Natural Science Edition)
基金
国家自然科学基金重点项目(20436020)
广东省自然科学基金资助项目(05006597)
关键词
超高静压
传压介质
压致升温
热损失
high hydrostatic pressure
pressure-transmitting fluid
compression heating
heat loss