摘要
目的:对二丁酰环磷腺苷钙及其冻干粉针的高效液相色谱法测定含量进行研究。方法:采用高效液相色谱法。结果:回收率为99.4%,RSD为0.45%。结论:该方法精密度良好,重现性好,操作简便、快速,可很好地测定二丁酰环磷腺苷钙及冻干粉针的含量。
Objective: To study the quantitative determination of the calcium dibutyryladenosine cyclophosphate and lyophilized powder for injection using high-performance liquid chromatography(HPLC). Methods: Determined the content using HPLC. Results: The Recovery rate was 99.4%, RSD was 0.45%. Conclusion: HPLC is fine in precision, highly reproducible, ready to be used, instant. It may determine the content of calcium dibutyryladenosine cyclophosphate and lyophilized powder for injection with high quality.
出处
《海南医学院学报》
CAS
2008年第1期19-21,共3页
Journal of Hainan Medical University
关键词
蛋白激酶
化学
药物
色谱法
高压液相
Protein kinase
Chemistry, drug
Chromatography, high-performance liquid